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CAS No 26299-14-9 , Pyridinium chlorochromate

  • Name: Pyridinium chlorochromate
  • Synonyms: PCC;Pyridinium chlorochromate;
  • CAS Registry Number:
  • Transport: UN 1479 5
  • Melting Point: 205 ºC
  • Water Solubility: soluble
  • Safety Statements: R43;R49;R50/53;R8
  • Hazard Symbols: O: Oxidizing agent;N: Dangerous for the environment;T: Toxic;
  • EINECS: 247-595-5
  • Molecular Weight: 215.55
  • InChI: InChI=1/C5H5N.ClH.Cr.3O/c1-2-4-6-5-3-1;;;;;/h1-5H;1H;;;;/rC5H5N.ClCrO3/c1-2-4-6-5-3-1;1-2(3,4)5/h1-5H;/q;-1/p+1
  • Risk Statements: S17;S24;S37;S45;S53;S60;S61
  • Molecular Formula: C5H5N.HCrO3Cl
  • Molecular Structure:CAS No:26299-14-9 Pyridinium chlorochromate

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26299-14-9 Pyridinium chlorochromate

  • Chemical Name: Pyridinium chlorochromate Chemical Type: Pharma Intermediates Catalog No: AC-22251 CASNO: 26299-14-9 Molecular Formula: C5H5N.HCrO3Cl Molecular Weight: 136.45 Purity: 98% welcome: sales(at)achemo(dot)com
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References of Pyridinium chlorochromate
Title: Pyridinium Chlorochromate
CAS Registry Number: 26299-14-9
CAS Name: Chlorotrioxochromate(1-), hydrogen, compd with pyridine (1:1)
Synonyms: PCC
Molecular Formula: C5H6ClCrNO3
Molecular Weight: 215.56
Percent Composition: C 27.86%, H 2.81%, Cl 16.45%, Cr 24.12%, N 6.50%, O 22.27%
Literature References: Oxidizing agent for the efficient conversion of primary or secondary alcohols to carbonyl compounds. Prepn: R. J. Meyer, H. Best, Z. Anorg. Allg. Chem. 22, 192 (1899); J. Bernard, M. Camelot, C.R. Hebd. Seances Acad. Sci. 258, 5881 (1964); and use as an oxidant: E. J. Corey, J. W. Suggs, Tetrahedron Lett. 1975, 2647. Improved prepn: S. Agarwal et al., Tetrahedron 46, 4417 (1990). Oxidation, ring enlargement of furans to pyranones: G. Piancatelli et al., Tetrahedron Lett. 1977, 2199; oxidation of tertiary allylic alcohols: W. G. Dauben, D. M. Michno, J. Org. Chem. 42, 682 (1977). Role in oxidative cationic cyclization: E. J. Corey, D. L. Boger, Tetrahedron Lett. 1978, 2461. Review: G. Piancatelli et al., Synthesis 1982, 245-258.
Properties: Orange-yellow solid, mp 205° (dec). Insol in dichloromethane.
Melting point: mp 205° (dec)
Use: Oxidizing agent in organic synthesis.