Home > Name List By 5 > 5,10b:11,4b-Bis(iminoethano)dibenzo[c,h][2,6]naphthyridine,5,6,11,12-tetrahydro-13,18-dimethyl-, (4bS,5R,10bS,11R)-

CAS No 595-05-1 , 5,10b:11,4b-Bis(iminoethano)dibenzo[c,h][2,6]naphthyridine,5,6,11,12-tetrahydro-13,18-dimethyl-, (4bS,5R,10bS,11R)-

  • Name: 5,10b:11,4b-Bis(iminoethano)dibenzo[c,h][2,6]naphthyridine,5,6,11,12-tetrahydro-13,18-dimethyl-, (4bS,5R,10bS,11R)-
  • Synonyms: [4bS-(4ba,5a,10ba,11a)]-5,6,11,12-Tetrahydro-13,18-dimethyl-5,10b:11,4b-bis(iminoethano)dibenzo[c,h][2,6]naphthyridine; (+)-Calycanthine; NSC 99016;5,10b:11,4b-Bis(iminoethano)dibenzo[c,h][2,6]naphthyridine,5,6,11,12-tetrahydro-13,18-dimethyl-, (4bS,5R,10bS,11R)-;d-Calycanthine;Calycanthine(6CI,7CI,8CI);5,10b:11,4b-Bis(iminoethano)dibenzo[c,h][2,6]naphthyridine,5,6,11,12-tetrahydro-13,18-dimethyl-, [4bS-(4ba,5a,10ba,11a)]-;
  • CAS Registry Number:
  • Flash Point: 310.3°C
  • Boiling Point: 531.8°Cat760mmHg
  • Density: 1.29g/cm3
  • Refractive index: 1.711
  • Flash Point: 310.3°C
  • EINECS: 209-857-7
  • Molecular Weight: 346.47
  • InChI: InChI=1/C22H26N4/c1-25-13-11-22-16-8-4-5-9-17(16)23-19(25)21(22)12-14-26(2)20(22)24-18-10-6-3-7-15(18)21/h3-10,19-20,23-24H,11-14H2,1-2H3/t19-,20-,21-,22-/m1/s1
  • Molecular Formula: C22H26 N4
  • Molecular Structure:CAS No:595-05-1 5,10b:11,4b-Bis(iminoethano)dibenzo[c,h][2,6]naphthyridine,5,6,11,12-tetrahydro-13,18-dimethyl-, (4bS,5R,10bS,11R)-

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595-05-1 Calycanthine

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References of 5,10b:11,4b-Bis(iminoethano)dibenzo[c,h][2,6]naphthyridine,5,6,11,12-tetrahydro-13,18-dimethyl-, (4bS,5R,10bS,11R)-
Title: Calycanthine
CAS Registry Number: 595-05-1
Molecular Formula: C22H26N4
Molecular Weight: 346.47
Percent Composition: C 76.27%, H 7.56%, N 16.17%
Literature References: In Calycanthus floridus L., C. glaucus Willd.; Chimonanthus praecox (L.) Link, Calycanthaceae. First isoln: Eccles, Proc. Am. Pharm. Assoc. 84, 382 (1888). Extraction procedure: Manske-Marion, Can. J. Res. 17B, 293 (1939). Structure: Woodward et al., Proc. Chem. Soc. London 1960, 76; Hamor et al., ibid. 78; Hamor, Robertson, J. Chem. Soc. 1962, 194. Configuration: Clayton et al., Tetrahedron 18, 1495 (1962). Synthesis of DL-form: Hendrickson et al., ibid. 20, 565 (1964); Hall et al., ibid. 23, 4131 (1967).
Properties: Crystals, mp 245° (evac tube). [a]D18 +684° (c = 1.2 in abs alc). uv max (95% ethanol): 250, 309 nm (log e 4.28, 3.80). Alkaline reaction to litmus. Freely sol in alc, chloroform; sol in ether, acetone, pyridine; slightly sol in water.
Melting point: mp 245° (evac tube)
Optical Rotation: [a]D18 +684° (c = 1.2 in abs alc)
Absorption maximum: uv max (95% ethanol): 250, 309 nm (log e 4.28, 3.80)
 
Derivative Type: Monohydrate
Properties: Orthorhombic bipyramidal crystals from water, mp 220°.
Melting point: mp 220°
 
CAUTION: Highly toxic. Can cause violent convulsions, paralysis, cardiac depression.